| | |
Position | 13C δ | 1H δ (Multiplicity, J Hz, Integral) | 13C δ | 1H δ (Multiplicity, J Hz, Integral) |
2 | 78.5 | 4.87 (d(br), 6.8, 2H) 4.73(*) | 82.2 | 4.73 (s, 2H) |
3 | 41.9 | — | 40.2 | — |
4 | 78.5 | 4.87 (d(br), 6.8, 2H) 4.73(*) | 82.2 | 4.73 (s, 2H) |
5 | 36.4 | 3.38 (s, 2H) | 63.9 | 3.42 (s, 2H) |
7 | 50.8 | 3.63 (s(br), 2H) | 63.9 | 3.42 (s, 2H) |
8 | 51.8 | 4.51, (s, 2H) | 63.1 | 3.54 (s, 2H) |
9 | 125.5 | — | 131.6 | — |
10 | 132.4 | 7.83 (d, 8.5, 2H) | 131.6 | 7.25 (d, 8.0, 2H) |
11 | 115.6 | 7.31 (d, 8.5, 2H) | 115.8 | 6.85 (d, 8.0, 2H) |
12 | 157.2 | — | 157.4 | — |
13 | 115.6 | 7.31 (d, 8.5, 2H) | 115.8 | 6.85 (d, 8.0, 2H) |
14 | 132.4 | 7.83 (d, 8.5, 2H) | 131.6 | 7.25 (d, 8.0, 2H) |
16 | 66.7 | 5.58 (m, 1H) | 67.6 | 5.16 (m, 1H) |
17* | 56.5 | 5.06 (m, 1H) 4.60 (m, 1H) | 57.2 | 4.69 (dd, 4.4/10.9, 1H) 4.21 (d(br), 1H) |
19* | 61.0 | 5, 50 (m, 1H) 5.03 (m, 1H) | 62.0 | 4.69 (dd, 4.4/10.9, 1H) 5.17 (m, 1H) |
20 | 154.2 | — | 158.8 | — |
22 | 157.6 | — | 155.1 | — |
24 | 166.1 | — | 167.0 | — |
27 | 115.1 | — | 116.3 | — |
28 | 129.8 | 8.42 (d, 8.9, 2H) | 130.4 | 8.09 (d, 8.3, 2H) |
29 | 115.4 | 7.15 (d, 8.7, 2H) | 116.0 | 7.14(d, 8.4, 2H) |
30 | 163.6 | — | 164.9 | — |
31 | 115.4 | 7.15 (d, 8.7, 2H) | 116.0 | 7.14(d, 8.4, 2H) |
32 | 129.8 | 8.42 (d, 8.9, 2H) | 130.4 | 8.09 (d, 8.3, 2H) |
34 | 56.0 | 4.26 (s, 3H) | 56.1 | 3.91 (s, 3H) |
36 | 34.7 | 3.40 (dd, 14.2, 5.4, 1H) 3.26 (dd, 14.2, 7.8, 1H) | | |
37 | 53.4 | 4.93 (dd, 7.8, 5.3, 1H) | | |
39 | 174.9 | — | | |
41 | 32.0 | 2.84 (m) | | |
42 | 26.6 | 2.45 (m) | | |
43 | 54.4 | 4.03 (t, 6.4, 6.4, 1H) | | |
45 | 173.7 | — | | |
48 | 171.5 | — | | |
51 | 43.7 | 4.08 (d, 17.2, 1H) 4.03 (d, 17.2, 1H) | | |
52 | 175.8 | — | | |