Table 3
Assignments of 1H and 13C NMR chemical shifts of RBM-1 (ED-594) in DMSO-d6
| No. | 13C NMR | 1H NMR |
|---|---|---|
| 1 | 143.8 | |
| 1a | 130.6 | |
| 2 | 114.2 | 7.05 |
| 3 | 121.7 | 7.21 |
| 4 | 115.4 | 8.68 |
| 5 | 166.4 ∗∗ | |
| 5a | 117.6 ∗ | |
| 5b | 119.6 | |
| 5c | 123.1 | |
| 7 | 166.3 ∗∗ | |
| 8 | 117.4 | 8.70 |
| 8a | 123.0 | |
| 8b | 117.5 | |
| 8c | 116.5 ∗ | |
| 9 | 121.3 | 7.32 |
| 10 | 110.7 | 7.25 |
| 11 | 143.1 | |
| 12a | 130.5 | |
| 13a | 129.5 | |
| 13b | 129.9 | |
| CHO | 160.6 | 8.44 |
| 1′ | 85.3 | 7.14 |
| 2′ | 72.3 | 3.78 |
| 3′ | 77.8 | 3.44 |
| 4′ | 68.8 | 3.95 |
| 5′ | 79.8 | 3.68 |
| 6′ | 58.8 | 4.06, 3.87 |
| 1" | 99.5 | 5.40 |
| 2" | 73.0 | 3.62 |
| 3" | 75.7 | 3.45 |
| 4" | 71.4 | 3.52 |
| 5" | 75.4 | 4.06 |
| 6" | 170.2 | |
| 6-NH | 10.8 | |
| 1-OH | 10.4 | |
| 12-NH | 11.0 | |
| OH | 5.98, 5.87, 5.28, 4.97 |
-
∗, ∗∗: may be interchanged.