No. | 13C NMR | 1H NMR |
---|---|---|
1 | 143.7 | |
1a | 130.5 | |
2 | 113.9 | 7.02 |
3 | 121.4 | 7.19 |
4 | 115.7 | 8.76 |
5 | 168.5 ∗∗ | |
5a | 117.3 ∗ | |
5b | 119.3 | |
5c | 123.3 | |
7 | 168.4 ∗∗ | |
8 | 117.6 | 8.77 |
8a | 123.2 | |
8b | 117.3 | |
8c | 117.1 ∗ | |
9 | 121.0 | 7.30 |
10 | 110.6 | 7.22 |
11 | 143.1 | |
12a | 130.5 | |
13a | 129.0 | |
13b | 129.5 | |
1′ | 85.2 | 7.12 |
2′ | 72.4 | 3.78 |
3′ | 77.9 | 3.43 |
4′ | 68.8 | 3.96 |
5′ | 79.8 | 3.68 |
6′ | 59.0 | 4.04, 3.86 |
1" | 99.6 | 5.37 |
2" | 73.0 | 3.61 |
3" | 75.8 | 3.45 |
4" | 71.5 | 3.50 |
5" | 75.3 | 4.01 |
6" | 170.4 | |
6-NH2 | 4.96 | |
1-OH | 10.4 | |
12NH | 10.8 | |
OH | 5.95, 5.81, 5.28, 4.96 |
∗, ∗∗: may be interchanged.