Table 4
Assignments of 1H and 13C NMR chemical shifts of RBM-2 (ED-595) in DMSO-d6
| No. | 13C NMR | 1H NMR |
|---|---|---|
| 1 | 143.7 | |
| 1a | 130.5 | |
| 2 | 113.9 | 7.02 |
| 3 | 121.4 | 7.19 |
| 4 | 115.7 | 8.76 |
| 5 | 168.5 ∗∗ | |
| 5a | 117.3 ∗ | |
| 5b | 119.3 | |
| 5c | 123.3 | |
| 7 | 168.4 ∗∗ | |
| 8 | 117.6 | 8.77 |
| 8a | 123.2 | |
| 8b | 117.3 | |
| 8c | 117.1 ∗ | |
| 9 | 121.0 | 7.30 |
| 10 | 110.6 | 7.22 |
| 11 | 143.1 | |
| 12a | 130.5 | |
| 13a | 129.0 | |
| 13b | 129.5 | |
| 1′ | 85.2 | 7.12 |
| 2′ | 72.4 | 3.78 |
| 3′ | 77.9 | 3.43 |
| 4′ | 68.8 | 3.96 |
| 5′ | 79.8 | 3.68 |
| 6′ | 59.0 | 4.04, 3.86 |
| 1" | 99.6 | 5.37 |
| 2" | 73.0 | 3.61 |
| 3" | 75.8 | 3.45 |
| 4" | 71.5 | 3.50 |
| 5" | 75.3 | 4.01 |
| 6" | 170.4 | |
| 6-NH2 | 4.96 | |
| 1-OH | 10.4 | |
| 12NH | 10.8 | |
| OH | 5.95, 5.81, 5.28, 4.96 |
-
∗, ∗∗: may be interchanged.