Table 5

13C chemical shift data for OA, 21-OH OA, and compound D

CarbonOA21-OH OACompound D
175.2674.9376.83
2
3164.08163.80166.75
4113.31113.03113.48
5155.39155.42158.33
6128.13127.32128.78
7138.41139.34141.19
837.8337.4939.19
945.7745.0847.08
1037.5437.2640.14
1120.1820.4621.07
1230.5730.3131.28
1347.2047.5348.42
1448.4447.8849.46
1523.2522.8924.13
1630.0930.0131.26
1795.9994.2395.10
1814.0813.4714.35
1915.4814.7315.78
20203.10205.80205.53
2126.4066.6373.54
G-15-a 103.89
G-274.90
G-377.54
G-473.54
G-575.92
G-6176.18
Ac(CH3)21.0919.6920.97
Ac(CO)170.24170.57172.61
  • 5-a  Carbon number of glucuronic acid moiety.