TABLE 3
Method validation in human urine samples
LOD
LOQ
Accuracy
Mean Retention Time ± S.D.
pmol/ml (μg/l)
pmol/ml (μg/l)
%
min
BPA
5 (1.14)
15 (3.42)
92-121
6.77 ± 0.06 (
n
= 55)
BPA-gluc
25
a
(10.1)
65 (26.26)
90-120
8.98 ± 0.05 (
n
= 33)
↵
a
LOD in water 0.9 pmol/ml.