Labela | SVA and CoASHb | SVA-CoA | P1-CoA | Simvastatin | M1 | ||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
1H | 13C | 1H | 13C | 1H | 13C | 1H | 13C | 1H | 13C | ||||||
2 | 178.5 | 197.9 | 190.0 | 172.0 | 172.3 | ||||||||||
3 | 2.28, 2.39 | 43.9 | 2.71, 2.77 | 50.8 | 6.22 | 129.9 | 2.52, 2.71 | 37.7 | 2.35, 2.85 | 38.7 | |||||
4 | 4.08 | 67.8 | 4.21 | 66.8 | 6.90 | 142.6 | 4.24 | 61.9 | 4.19 | 62.8 | |||||
5 | 1.55 | 43.8 | 1.60 | 43.4 | 2.35 | 40.0 | 1.74, 1.91 | 35.2 | 1.49, 2.24 | 37.5 | |||||
6 | 3.69 | 70.3 | 3.63 | 69.9 | 3.57 | 71.0 | 4.61 | 76.7 | 4.19 | 77.8 | |||||
7 | 1.27, 1.54 | 34.4 | 1.17, 1.54 | 32.9 | 1.17, 1.55 | 34.1 | 1.35, 1.82 | 32.7 | 1.36, 1.85 | 32.6 | |||||
8 | 1.40 | 24.5 | 1.34 | 24.4 | 1.37 | 24.7 | 1.39, 1.49 | 23.9 | 1.41, 1.49 | 24.6 | |||||
a′ | 2.58 | 23.1 | 3.00 | 27.9 | 3.04 | 27.6 | |||||||||
b′ | 3.31 | 42.5 | 3.31 | 38.6 | 3.32 | 38.8 | |||||||||
c′ | 172.8 | 172.7 | 172.7 | ||||||||||||
d′ | 2.45 | 35.3 | 2.41 | 35.2 | 2.43 | 35.3 | |||||||||
e′ | 3.46 | 35.1 | 3.45 | 35.1 | 3.46 | 35.1 | |||||||||
f′ | 174.3 | 174.4 | 174.4 | ||||||||||||
g′ | 4.05 | 73.9 | 4.06 | 73.5 | 4.08 | 73.5 | |||||||||
h′ | 38.8 | 38.7 | 38.7 | ||||||||||||
h′-Me | 0.82, 1.02 | 18.3, 20.8 | 0.83, 1.05 | 18.1, 21.0 | 0.82, 1.05 | 18.1, 20.9 | |||||||||
i′ | 3.59, 3.96 | 71.8 | 3.56, 3.98 | 71.8 | 3.57, 3.99 | 71.7 | |||||||||
R1 | 6.13 | 87.4 | 6.12 | 87.1 | 6.14 | 87.1 | |||||||||
R2, R4 | 4.76, 4.92 | 74.1, 74.6 | 4.79, 4.86 | 74.1, 74.4 | 4.79, 4.92 | 74.1, 74.5 | |||||||||
R3 | 4.52 | 83.3 | 4.50 | 83.4 | 4.50 | 83.4 | |||||||||
R5 | 4.28 | 64.9 | 4.24 | 65.1 | 4.23, 4.30 | 64.9 | |||||||||
A2 | 8.22 | 150.3 | 8.20 | 152.4 | 8.20 | 152.4 | |||||||||
A6 | 8.62 | 140.6 | 8.57 | 139.6 | 8.59 | 139.7 |
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