TABLE 2

1H and 13C NMR chemical shifts of dihydrotestosterone diglucuronide

The experiments were conducted at 25°C using DMSO-d6 as a solvent.


Carbon No.

1H

13C
1 1.25, 1.94 37.6
2 2.10, 2.41 37.3
3 210.2
4 1.88, 2.28 43.9
5 1.44 45.8
6 1.26 28.0
7 0.83, 1.60 30.6
8 1.34 34.4
9 0.67 53.0
10 35.0
11 1.29, 1.46 20.1
12 0.95, 1.89 35.9
13 42.3
14 0.87 49.7
15 1.15, 1.46 22.7
16 1.48, 1.84 28.5
17 3.45 88.9
18 0.68 10.9
19 0.97 10.7
1′ 4.37 102.0
2′ 3.25 82.3
3′ 3.40 75.2
4′ 3.35 71.0
5′ 3.58 74.8
6′ 169.7
1″ 4.43 104.5
2″ 3.04 74.8
3″ 3.20 75.1
4″ 3.29 71.4
5″ 3.57 76.0
6″

169.9