TABLE 1

Accuracy and repeatability of the analytical method based on quality control samples analyzed (n = 8)




Level

Accuracy

Repeatability



Accuracy

Repeatability
ng/ml % RSD% % RSD%
Fexofenadine 186 98-102 1.8-3.3 92 6.2
    Plasma 37 90-97 1.7-6.8 Bile 94 5.5
3.7 92-100 1.7-4.4 99 14
0.59 79-121 3.7-11.4
Verapamil 196 97-99 1.6-2.8 96 6.8
    Plasma 39 93-114 1.1-13 Bile 94 4.3
3.9 88-99 2.9-10 96 13
0.61 79-100 4.5-21
Antipyrine 185 92-113 6.6-39
    Plasma 93 87-117 17-21

37
73-121
12-48