No. | M-15a | M-16a |
---|---|---|
1 | 1.90 (m) | 2.05 (dd,10.6, 9.3) |
2 | 1.87 (m, α) | 1.75 (m, α) |
1.58 (m, β) | 1.92 (m, β) | |
3 | 1.76 (m, α) | 1.36 (m, α) |
1.35 (m, β) | 1.85 (1H, m, β) | |
4 | 1.70 (m) | 1.80 (m) |
6 | 1.30 (dd,14.4,7.2, α) 2.24 (dd, 16.2, 14.4, β) | 1.53 (d,14.6,α) 2.23 (d,14.6, β) |
7 | 1.48 (m) | 2.39 (m) |
8 | ||
9 | 2.28 (d, 14.4, α) 1.78 (m, β) | 3.10 (d, 11.3, α)) 2.52 (d, 11.3, β) |
11 | 1.54 (m) | 1.90 (m) |
12 | 0.98 (d,6.0) | 0.92 (d, 7.2) |
13 | 0.94 (d, 6.4) | 0.99 (d, 6.6) |
14 | 3.30 (br.s) | 3.30 (d, 10.7, a) |
3.30 (br.s) | 3.41 (d, 10.7, b) | |
15 | 1.01 (d, 6.4) | 0.91 (d, 7.2) |
↵a Recorded at 600 MHz in CD3OD.