| | | ppm |
Anacetrapib: [M + H]+ = 638.1755; C30H26F10NO3 (δ = +1.17 ppm) | 325.1200 | [C18H17OF4]+ | −3.09 |
| 314.0601 | [C12H10O2NF6]+ | −2.95 |
| 283.0731 | [C15H11OF4]+ | −3.37 |
M1: [M − H]− = 622.1429; C29H22F10NO3 (δ = −2.65 ppm) | 578.1536 | [C28H22ONF10]− | −1.94 |
| 324.1010 | [C17H14ONF4]− | −2.16 |
| 312.0457 | [C12H8O2NF6]− | −2.47 |
| 292.0396 | [C12H7O2NF5]− | −2.20 |
M2: [M − H]− = 638.1392; C29H22F10NO4− (δ = −0.41 ppm) | 594.1486 | [C28H22O2NF10]− | −1.74 |
| 325.0850 | [C17H13O2F4]− | −2.20 |
| 312.0458 | [C12H8O2NF6]− | −2.15 |
| 305.0788 | [C17H12O2F3]− | −2.26 |
| 292.0396 | [C12H7O2NF5]− | −2.20 |
M3: [M − H]− = 638.1392; C29H22F10NO4− (δ = −0.41 ppm) | 620.1278 | [C29H20O3NF10]− | −1.77 |
| 594.1486 | [C28H22O2NF10]− | −1.74 |
| 576.1381 | [C28H20ONF10]− | −1.68 |
| 536.1068 | [C25H16ONF10]− | −1.81 |
| 312.0457 | [C12H8O2NF6]− | −2.47 |
| 292.0396 | [C12H7O2NF5]− | −2.20 |