TABLE 1

Accurate mass data for LY654322 and its metabolite M25

Compound	Ion	Composition	Measured Mass	Calculated Mass	mDa^{^a}	ppm^{^b}
LY654322	563	C₃₁H₄₀N₆O₃F	563.3113	563.3146	−3.3	−5.9
	488	C₂₈H₃₁N₅O₂F	488.2449	488.2462	−1.3	−2.6
	398	C₂₁H₂₅N₅O₂F	398.1989	398.1992	−0.3	−0.8
	344	C₁₈H₂₆N₅O₂	344.2104	344.2087	1.7	5.1
	179	C₈H₁₁N₄O	179.0923	179.0933	−1	−5.5
M25	598	C₃₃H₃₄N₇O₂F₂	598.2723	598.2742	−1.9	−3.2
	379	C₂₀H₂₀N₆OF	379.1683	379.1683	0	0
	220	C₁₃H₁₅NOF	220.1133	220.1138	−0.5	−2.3
	192	C₁₂H₁₅NF	192.1187	192.1189	−0.2	−1.0
	160	C₇H₆N₅	160.0619	160.0623	−0.4	−2.5