X-ray crystallography data collection statistics
Values in parentheses correspond to the highest resolution shell.
| Crystal Sample | |||
|---|---|---|---|
| mNAT-I | mNAT-II | mNAT (Merged) | |
| X-ray source | ID 14-1 | ID 23-2 | |
| Crystal system | Triclinic | Triclinic | Triclinic |
| Unit-cell parameters (Å, °) | |||
| a, b, c, Å | 91.07, 135.02, 147.48 | 91.54, 135.83, 147.84, | |
| α, β, γ, ° | 78.27, 77.77, 89.96 | 78.22, 77.89, 89.97 | |
| Maximum resolution, Å | 2.9 | 3.2 | 3.0 |
| Mosaicity, ° | 1.0 | 1.0 | 1.0 |
| Molecules per asymmetric unit | 4 | 4 | 4 |
| Matthews coefficient, Å3/Da | 2.89 | 2.93 | |
| Space group | P1 | P1 | P1 |
| Wavelength, Å | 0.934 | 0.975 | |
| No. of observed reflections | 219,268 (20,892) | 223,954 (24,999) | 338,761 (41,810) |
| No. of unique reflections | 133,319 (16,784) | 78,529 (10,857) | 112,209 (16,428) |
| Resolution limits, Å | 51.1–2.9 | 50.0–3.2 | 50 0.0–3.20 |
| Redundancy | 1.6 (1.2) | 2.8 (2.2) | 3.0 (2.5) |
| Completeness, % | 89.8 (77.3) | 69.5 (65.1) | 81.8 (81.7) |
| Rpim, % | 5.6 (14.0) | 14.3 (68.9) | 17.5 (63.4) |
| I/σ | 9.6 (3.6) | 6.3 (1.4) | 7.0 (4.2) |