TABLE 1
Gradient elution for the optimal separation of raloxifene, its glucuronides, and haloperidol
Time
Mobile Phase B
Flow
%
ml/min
0.25 min
10
0.65
0.50 min
20
0.65
1.00 min
30
0.65
1.25 min
50
0.65
1.70 min
50
0.65
1.75 min
10
0.65