C/H Number | M12a/M12b | M13a/M13b | ||||
---|---|---|---|---|---|---|
δH | J-H,H Values | δC | δH | J-H,H Values | δC | |
C-1/H-1 | 1.50(m) | 29.52/29.92 | 1.23(m)/1.43(m) | 29.68/29.22 | ||
1.84(m) | 1.71(m)/1.82(m) | |||||
C-2/H-2 | 4.76(dd) | 5.5, 5.5 | 76.94 | 4.74(dd) | 5.5, 5.5 | 76.74 |
C-3/H-3 | 1.72(d) | 11.7 | 39.20 | 1.67(d) | 11.5 | 39.00 |
2.34(dd) | 5.4, 11.7 | 2.33(dd) | 5.5, 11.5 | |||
C-4/H-4 | 2.79(d) | 4.4 | 42.42 | 2.77(d) | 5 | 42.19 |
C-5/H-5 | 1.99(d) | 12.0 | 42.33 | 1.92(d) | 11.7 | 42.07/41.98 |
C-6/H-6 | 4.78(d) | 5.7 | 78.11/77.9 | 4.73(d) | 6.0 | 77.66/77.60 |
C-7/H-7 | 2.13(d) | 11.6 | 37.19 | 2.07(d) | 11.6 | 37.12 |
2.53(dd) | 5.8, 11.6 | 2.51(dd)/2.49(dd) | 5.5, 11.6 | |||
C-8 | 90.02/90.22 | 90.05/89.96 | ||||
C-9 | 45.73 | 45.55/45.47 | ||||
C-10/H-10 | 2.50(m) | 40.98 | 2.04(m)/1.92(m) | 38.89 | ||
C-11/H-11 | 2.0(dd)/1.82(dd) | 11.7, 12.1/11.4, 11.7 | 40.52/39.63 | 1.22(dd)/1.65(dd) | 10.5, 11.5 | 40.75/40.38 |
2.24(dd)/2.08(dd) | 6.0, 12.1/5.3, 11.7 | 1.98(dd)/2.23(dd) | 5.5, 11.5 | |||
C-12/H-12 | 5.39(dd)/5.20(dd) | 5.5, 10.5 | 76.55/76.83 | 5.20(dd) | 5.5, 10.5 | 75.46/75.16 |
C-13 | 169.99/169.38 | 135.7/137.15 | ||||
C-14 | 6.56(s)/6.79(s) | 117.31/118.29 | 7.90(s) | 147.46/147.33 | ||
C-15/H-15 | 171.38/171.23 | 6.52(s)/6.62(s) | 99.00 | |||
C-16/H-16 | 6.46(s)/6.71(s) | 99.49/98.5 | 170.82 | |||
C-17 | 177.08/176.75 | 176.77 | ||||
C-18 | 176.03 | 175.88 | ||||
C-20/3H | 1.09(s)/1.06(s) | 16.21/15.94 | 0.98(s)/0.99(s) | 15.87/15.75 |
C/H, Carbon/Hydrogen; d, doublet; dd, doublet doublet; m, multiplet; s, singlet.