TABLE 1

1H and 13C NMR chemical shift assignments of N-glucuronide of BMS-204352 Atom labels are shown in Fig. 4.


Carbon Number

H1 Shift

Carbon Shift
2 176.78
3 91.63
4
5 143.54
6 7.36 108.87
7
8 7.314 120.72
9 7.26 126.01
12
13 154.4
14 6.85 114.2
15 7.33 130.82
16 125.9
17 7.68 125.8
18
21 3.54 56.03
1′ 5.34 82.85
2′ 4 69.26
3′ 3.59 78
4′ 3.78 71.8
5′ 3.91 74
6′

167.65