1H and 13C NMR chemical shifts of dihydrotestosterone diglucuronide
The experiments were conducted at 25°C using DMSO-d6 as a solvent.
Carbon No. | 1H | 13C |
---|---|---|
1 | 1.25, 1.94 | 37.6 |
2 | 2.10, 2.41 | 37.3 |
3 | 210.2 | |
4 | 1.88, 2.28 | 43.9 |
5 | 1.44 | 45.8 |
6 | 1.26 | 28.0 |
7 | 0.83, 1.60 | 30.6 |
8 | 1.34 | 34.4 |
9 | 0.67 | 53.0 |
10 | 35.0 | |
11 | 1.29, 1.46 | 20.1 |
12 | 0.95, 1.89 | 35.9 |
13 | 42.3 | |
14 | 0.87 | 49.7 |
15 | 1.15, 1.46 | 22.7 |
16 | 1.48, 1.84 | 28.5 |
17 | 3.45 | 88.9 |
18 | 0.68 | 10.9 |
19 | 0.97 | 10.7 |
1′ | 4.37 | 102.0 |
2′ | 3.25 | 82.3 |
3′ | 3.40 | 75.2 |
4′ | 3.35 | 71.0 |
5′ | 3.58 | 74.8 |
6′ | 169.7 | |
1″ | 4.43 | 104.5 |
2″ | 3.04 | 74.8 |
3″ | 3.20 | 75.1 |
4″ | 3.29 | 71.4 |
5″ | 3.57 | 76.0 |
6″ |
| 169.9 |