TABLE 1

Data collection and refinement statistics for crystals of variant hAOX1-S1271L

hAOX1-S1271La
Data collection
 Space groupP42212
 Cell dimensions
a = b, c (Å)147.40, 131.70
 Resolution (Å)49.15–3.41 (3.68–3.41)
Rmerge0.30 (1.75)
I / s(I)9.50 (2.20)
 Completeness (%)100.00 (100.00)
 Redundancy10.8 (11.1)
Refinement
 Resolution (Å)3.41
 No. of reflections20403 (4115)
Rwork / Rfree18.7 / 24.6
No. of atoms
 Protein9995
 Ligand/ion13
Water52
B-factors
 Protein73.90
 Ligand/ion73.70
 Water35.60
RMS deviations
 Bond lengths (Å)0.014
 Bond angles (°)1.545
  • RMS, root-mean-square deviation.

  • a Values in parentheses are for highest-resolution shell